Ethanol → N-[[(4-Nitrophenyl)methoxy]carbonyl]-L-isoleucine
반응식
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][O:11][C:12](=[O:23])OC2C=CC([N+]([O-])=O)=CC=2)=[CH:6][CH:5]=1)([O-:3])=[O:2].[NH2:24][C@H:25]([C:30]([OH:32])=[O:31])[C@H:26]([CH2:28][CH3:29])[CH3:27].C(N(CC)CC)C.C(O)C>O>[N+:1]([C:4]1[CH:5]=[CH:6][C:7]([CH2:10][O:11][C:12]([NH:24][C@H:25]([C:30]([OH:32])=[O:31])[C@H:26]([CH2:28][CH3:29])[CH3:27])=[O:23])=[CH:8][CH:9]=1)([O-:3])=[O:2]참가 물질
6
실험 절차
The title compound is prepared by the procedure of Example 255 using 14.73 g of product from Example 254, 6.07 g of L-isoleucine, 12.73 ml of triethylamine and 556 ml of 4:1 ethyl alcohol:water to give 3.52 g of the desired product.
출처 및 근거
- ORD 기록
- ord-1849cdd34ca7460f86457d497ba7c0d0
- 출처 데이터셋
- uspto-grants-1997_04
- 특허 번호
- US05623081
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