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Diethyl Ether → HCID 67199887, 화합물

HRID 550319
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인쇄 미리보기

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HRID 550319 반응식
[CH3:1][N:2]([CH3:15])[C:3]1[CH:8]=[CH:7][C:6]([C:9]2[CH:14]=[CH:13][N:12]=[CH:11][CH:10]=2)=[CH:5][CH:4]=1.[CH2:16]([I:18])[CH3:17].C(OCC)C>C(#N)C>[I-:18].[CH3:1][N:2]([CH3:15])[C:3]1[CH:4]=[CH:5][C:6]([C:9]2[CH:10]=[CH:11][N+:12]([CH2:16][CH3:17])=[CH:13][CH:14]=2)=[CH:7][CH:8]=1
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참가 물질

5

반응물 3

HCID 3283Diethyl EtherHCID 6340IodoethaneHCID 227783N,N-dimethyl-4-(pyridin-4-yl)aniline

생성물 1

HCID 67199887HCID 67199887, 화합물수율 18%

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

IDT321. Was prepared by refluxing N,N-dimethyl-4-(pyridine-4-yl) aniline (II) in acetonitrile in the presence of ethyl iodide. Upon cooling diethyl ether was added and the product crystallized resulting in a 18% yield of 4-(4-(dimethylamino)phenyl)-1-ethylpyridinium iodide (IDT321) (IV).

후처리

  1. customWas prepared
  2. additionwas added
  3. customthe product crystallized

출처 및 근거

ORD 기록
ord-8ac69fa2f8b74e39863302a8ef815c00
출처 데이터셋
uspto-grants-2011_05
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07947255B2

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