Acetic Anhydride → N-[2-(4,5-Dimethyl-thiophen-2-yl)-ethyl]-acetamide

반응식

[CH3:1][C:2]1[CH:3]=[C:4]([CH2:8][CH2:9][NH2:10])[S:5][C:6]=1[CH3:7].[C:11](OC(=O)C)(=[O:13])[CH3:12]>>[CH3:1][C:2]1[CH:3]=[C:4]([CH2:8][CH2:9][NH:10][C:11](=[O:13])[CH3:12])[S:5][C:6]=1[CH3:7]

참가 물질

반응물 2

HCID 7918Acetic Anhydride

HCID 530135252-(4,5-Dimethyl-thiophen-2-yl)-ethylamine

생성물 1

HCID 59663060N-[2-(4,5-Dimethyl-thiophen-2-yl)-ethyl]-acetamide수율 79%

실험 절차

In close analogy to the procedure described above, 2-(4,5-Dimethyl-thiophen-2-yl)-ethylamine is reacted with acetic anhydride to provide the title compound.

출처 및 근거

ORD 기록: ord-9b73af21af4140ac8769ff493a85cb48
출처 데이터셋: uspto-grants-2011_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07947689B2

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