Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → HCID 178444542, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | HCID 178444557 | HCID 178444557 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | HCID 178444542 | HCID 178444542 | — |
반응 단계
20 mL of thionyl chloride was added dropwise to a mixture containing 20.0 g (0.1 mol) of trans-4-pentylcyclohexanecarboxylic acid represented by the following formula (b-i), 0.5 mL of pyridine and 300 mL of toluene in a nitrogen atmosphere, and the mixture was stirred under heating to 80° C. or less for 1 hour. The solvent was distilled off under reduced pressure to provide trans-4-pentylcyclohexanecarboxylic acid chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08048335B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-ca2f9cd410f44863bb2746a888088958 |
| 출처 메모 | uspto-grants-2011_11 |