Hydrochloric Acid → Methyl 2-amino-3-(3-hydroxyphenyl)propanoate

HRID 553817

반응식

HRID 553817 반응식
[CH:1]1[CH:6]=[C:5]([OH:7])[CH:4]=[C:3]([CH2:8][CH:9]([NH2:13])[C:10]([OH:12])=[O:11])[CH:2]=1.Cl.[CH3:15]O>>[CH3:15][O:11][C:10](=[O:12])[CH:9]([NH2:13])[CH2:8][C:3]1[CH:2]=[CH:1][CH:6]=[C:5]([OH:7])[CH:4]=1

참가 물질

4

반응물 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 130523-Tyrosine, DL-

생성물 1

HCID 22386100Methyl 2-amino-3-(3-hydroxyphenyl)propanoate

실험 절차

DL-m-Tyrosine (1 g) was stirred in a 3M solution of HCl in MeOH (10 ml) for 2 h at RT The solvent was removed and HV drying afforded 1.43 g of the desired compound.

후처리

  1. customwas removed
  2. customHV drying

출처 및 근거

ORD 기록
ord-e4efb3f233254d498547e13133f49e9c
출처 데이터셋
uspto-grants-2011_11
특허 번호
US08048881B2

연결된 노트

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