Benzidine → N,N,N',N'-Tetrakis(4-amino-phenyl)benzidine

HRID 5540

반응식

[CH:1]1[C:6]([NH2:7])=[CH:5][CH:4]=[C:3]([NH2:8])[CH:2]=1.[C:9]1([C:16]2[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=2)[CH:15]=[CH:14][C:12](N)=[CH:11][CH:10]=1>>[NH2:7][C:6]1[CH:5]=[CH:4][C:3]([N:8]([C:3]2[CH:4]=[CH:5][C:6]([NH2:7])=[CH:1][CH:2]=2)[C:12]2[CH:11]=[CH:10][C:9]([C:16]3[CH:22]=[CH:21][C:19]([N:20]([C:16]4[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=4)[C:9]4[CH:15]=[CH:14][C:12]([NH2:8])=[CH:11][CH:10]=4)=[CH:18][CH:17]=3)=[CH:15][CH:14]=2)=[CH:2][CH:1]=1

참가 물질

반응물 2

HCID 7111Benzidine

HCID 7814P-Phenylenediamine

생성물 1

HCID 5130174N,N,N',N'-Tetrakis(4-amino-phenyl)benzidine

실험 절차

The same reaction as in Synthesis example 1 was carried out except for changing p-phenylenediamine used in Synthesis example 1 to benzidine to obtain 12 parts of orange tetrakis (p-aminophenyl)benzidine.

후처리

customThe same reaction
customas in Synthesis example 1

출처 및 근거

ORD 기록: ord-9589a48d34f74be29e906b317fd0389c
출처 데이터셋: uspto-grants-1993_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05245030

연결된 노트

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