반응식
[Cl:1][C:2]1[CH:7]=[C:6]([CH3:8])[CH:5]=[C:4]([Cl:9])[C:3]=1[OH:10].C1(=O)O[CH2:14][CH2:13][O:12]1.N1C=CN=C1>>[Cl:1][C:2]1[CH:7]=[C:6]([CH3:8])[CH:5]=[C:4]([Cl:9])[C:3]=1[O:10][CH2:14][CH2:13][OH:12]참가 물질
4
반응 조건
- 온도
- 150 °C
실험 절차
2,6-Dichloro-4-methylphenol (1 eq.), ethylene carbonate (1 eq.) and imidazole (0.5% loading) were combined and heated at 150° C. for 4 h to afford the title compound as a brown oil.
출처 및 근거
- ORD 기록
- ord-1ab1a93deda14501b292e7f6ce123d80
- 출처 데이터셋
- uspto-grants-2011_11
- 특허 번호
- US08063105B2
연결된 노트
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