Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromo-5-nitrobenzoic acid → (2-Bromo-5-nitrophenyl)methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromo-5-nitrobenzoic acid | HCID 243025 | — |
| 반응물 | Borane;tetrahydrofuran | HCID 2723981 | — |
| 생성물 | (2-Bromo-5-nitrophenyl)methanol | HCID 18671373 | — |
반응 단계
To 2-bromo-5-nitrobenzoic acid (5 g, 20 mmol) at 0° C. was added borane tetrahydrofuran complex (1 M in THF; 200 mL, 200 mmol), and the reaction was stirred at room temperature overnight. The mixture was quenched with 1N aqueous HCl to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08067445B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-10610fa9968e4d3ba8c45c75675bc868 |
| 출처 메모 | uspto-grants-2011_11 |