HRID563537

反应详情

EQUATION

反应方程式

HRID 563537 的结构方程式

PROCEDURE

实验过程

To 2-bromo-5-nitrobenzoic acid (5 g, 20 mmol) at 0° C. was added borane tetrahydrofuran complex (1 M in THF; 200 mL, 200 mmol), and the reaction was stirred at room temperature overnight. The mixture was quenched with 1N aqueous HCl to give the title compound.

WORKUP

后处理

  1. customThe mixture was quenched with 1N aqueous HCl