Ammonia → N-(3-Chlorophenyl)benzenemethanamine
반응식
C(C(C(C(O)=O)O)O)(O)=O.[Cl:11][C:12]1[CH:13]=[C:14]([NH:18][CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:15]=[CH:16][CH:17]=1.N>C(Cl)(Cl)Cl>[Cl:11][C:12]1[CH:13]=[C:14]([NH:18][CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:15]=[CH:16][CH:17]=1참가 물질
4
실험 절차
Next, (+)-(3-chlorophenyl)phenylmethylamine (+)tartrate (4.28 g) was suspended in chloroform (40 ml), and 28%-aqueous ammonia was added thereto to neutralize the mixture. Thereafter, the chloroform layer was separated therefrom. The extract was dried over anhydrous magnesium sulfate, and the solvent was removed by evaporation in vacuo, to give (+)-(3-chlorophenyl)phenylmethylamine (2.45 g) as a pale yellow oil.
후처리
- customThereafter, the chloroform layer was separated
- dry with materialThe extract was dried over anhydrous magnesium sulfate
- customthe solvent was removed by evaporation in vacuo
출처 및 근거
- ORD 기록
- ord-c26e0cf2cd824304818775200eedf1f3
- 출처 데이터셋
- uspto-grants-2001_01
- 특허 번호
- US06172228B2
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