반응식
[C:1](#[N:5])[CH2:2][C:3]#[N:4].[C:6](OCC)(OCC)([O:9][CH2:10][CH3:11])[CH2:7][CH3:8]>>[CH2:10]([O:9][C:6](=[C:2]([C:1]#[N:5])[C:3]#[N:4])[CH2:7][CH3:8])[CH3:11]참가 물질
3
실험 절차
16.41 g (249 mmol) of malononitrile and 43.8 g (249 mmol) of triethyl orthopropionate are refluxed for 4.5 hours. The reaction mixture is cooled to room temperature and distilled in vacuo.
후처리
- distillationdistilled in vacuo
출처 및 근거
- ORD 기록
- ord-5a7a2ebc62324adab460e8a1db82e678
- 출처 데이터셋
- uspto-grants-2001_01
- 특허 번호
- US06174884B1
연결된 노트
불러오는 중…