4-Decanone → tert-Butyl N'-(1-propyl-heptylidene)-hydrazinecarboxylate
반응식
[CH3:1][CH2:2][CH2:3][C:4](=O)[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[C:12]([O:16][C:17]([CH3:20])([CH3:19])[CH3:18])(=[O:15])[NH:13][NH2:14]>C1CCCCC1.CCCCCCC>[CH2:3]([C:4](=[N:14][NH:13][C:12]([O:16][C:17]([CH3:20])([CH3:19])[CH3:18])=[O:15])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[CH2:2][CH3:1]참가 물질
4
실험 절차
24.76 g (158 mmol) of 4-decanone and 20.94 g (158 mmol) of tert-butyl carbazate are heated for 90 minutes at 80° C. in 250 ml of cyclohexane/heptane mixture (1:1). After cooling, 39.71 g (93%) of a white solid are obtained by crystallization.
후처리
- temperatureAfter cooling
출처 및 근거
- ORD 기록
- ord-37087aa4fed64276a09e56a8bf9701c7
- 출처 데이터셋
- uspto-grants-2001_01
- 특허 번호
- US06174884B1
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