4-Decanone → tert-Butyl N'-(1-propyl-heptylidene)-hydrazinecarboxylate

HRID 566320

반응식

HRID 566320 반응식
[CH3:1][CH2:2][CH2:3][C:4](=O)[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[C:12]([O:16][C:17]([CH3:20])([CH3:19])[CH3:18])(=[O:15])[NH:13][NH2:14]>C1CCCCC1.CCCCCCC>[CH2:3]([C:4](=[N:14][NH:13][C:12]([O:16][C:17]([CH3:20])([CH3:19])[CH3:18])=[O:15])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[CH2:2][CH3:1]

참가 물질

4

반응물 2

HCID 122034-DecanoneHCID 70091tert-Butyl carbazate

생성물 1

HCID 72599202tert-Butyl N'-(1-propyl-heptylidene)-hydrazinecarboxylate수율 93%

시약·촉매·용매 1

HCID 21477393Cyclohexane heptane용매

실험 절차

24.76 g (158 mmol) of 4-decanone and 20.94 g (158 mmol) of tert-butyl carbazate are heated for 90 minutes at 80° C. in 250 ml of cyclohexane/heptane mixture (1:1). After cooling, 39.71 g (93%) of a white solid are obtained by crystallization.

후처리

  1. temperatureAfter cooling

출처 및 근거

ORD 기록
ord-37087aa4fed64276a09e56a8bf9701c7
출처 데이터셋
uspto-grants-2001_01
특허 번호
US06174884B1

연결된 노트

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