Sulfamide → HCID 178479209, 화합물

HRID 569276

반응식

HRID 569276 반응식
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].Cl.[Cl:7][CH2:8][CH2:9][C:10]#[N:11]>C(OCC)C>[ClH:7].[S:1]([NH:5][C:10](=[NH:11])[CH2:9][CH2:8][Cl:7])(=[O:3])(=[O:2])[NH2:4]

참가 물질

4

반응물 2

HCID 82267SulfamideHCID 867420433-Chloropropionitrile hydrogen chloride

생성물 1

HCID 178479209HCID 178479209, 화합물

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.

후처리

  1. additionTo a stirred suspension of 9.61 g
  2. filtrationthe product is filtered off
  3. washwashed twice with acetone
  4. customdried

출처 및 근거

ORD 기록
ord-3edc6a87650c40d881e2ef0137c4c5f3
출처 데이터셋
uspto-grants-1988_03
특허 번호
US04731479

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