Sulfamide → HCID 178479209, 화합물
반응식
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].Cl.[Cl:7][CH2:8][CH2:9][C:10]#[N:11]>C(OCC)C>[ClH:7].[S:1]([NH:5][C:10](=[NH:11])[CH2:9][CH2:8][Cl:7])(=[O:3])(=[O:2])[NH2:4]참가 물질
4
실험 절차
To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.
후처리
- additionTo a stirred suspension of 9.61 g
- filtrationthe product is filtered off
- washwashed twice with acetone
- customdried
출처 및 근거
- ORD 기록
- ord-3edc6a87650c40d881e2ef0137c4c5f3
- 출처 데이터셋
- uspto-grants-1988_03
- 특허 번호
- US04731479
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