Ammonia → Morpholine-4-carboxamide

HRID 574961

반응식

HRID 574961 반응식
[N:1]1([C:7](Cl)=[O:8])[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[NH3:10]>CO>[N:1]1([C:7]([NH2:10])=[O:8])[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1

참가 물질

4

반응물 2

HCID 222AmmoniaHCID 848104-Morpholinecarbonyl chloride

생성물 1

HCID 75088Morpholine-4-carboxamide

시약·촉매·용매 1

HCID 887Methanol용매2회

실험 절차

A solution of morpholine-4-carbonyl chloride (2.0 g) in methanol (10 mL) and 7 N NH3 in methanol (5 mL) was stirred at 45° C. overnight. The mixture was concentrated to give a solid, which was dried under vacuum.

후처리

  1. concentrationThe mixture was concentrated
  2. customto give a solid, which
  3. customwas dried under vacuum

출처 및 근거

ORD 기록
ord-bc64eee410bf4511854d76a992fb5970
출처 데이터셋
uspto-grants-2015_05
특허 번호
US09034875B2

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