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Hydrochloric Acid → (S)-methyl 2-((2-aminobutyl)amino)-2-oxoacetate hydrochloride

HRID 576697
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HRID 576697 반응식
[ClH:1].C(OC([NH:9][C@@H:10]([CH2:19][CH3:20])[CH2:11][NH:12][C:13](=[O:18])[C:14]([O:16][CH3:17])=[O:15])=O)(C)(C)C>O1CCOCC1>[ClH:1].[NH2:9][C@@H:10]([CH2:19][CH3:20])[CH2:11][NH:12][C:13](=[O:18])[C:14]([O:16][CH3:17])=[O:15]
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참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 90402569(S)-methyl 2-((2-((tert-butoxycarbonyl)amino)butyl)amino)-2-oxoacetate

생성물 1

HCID 90402534(S)-methyl 2-((2-aminobutyl)amino)-2-oxoacetate hydrochloride수율 100%

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

실험 절차

To an ice cold solution of 4M HCl in dioxane (20 mL) was added (S)-methyl 2-((2-((tert-butoxycarbonyl)amino)butyl)amino)-2-oxoacetate (1.3 g, 4.6 mmol). After 30 minutes, the reaction mixture was concentrated to provide a yellow foam (968 mg, 100%), which was used without further purification. MS (ESI): mass calcd. for C7H14N2O3, 174.1; m/z found, 175.2 [M+H]+.

후처리

  1. concentrationthe reaction mixture was concentrated

출처 및 근거

ORD 기록
ord-bda0854d96414bc7a4b7580f3d972256
출처 데이터셋
uspto-grants-2015_05
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US09040534B2

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