Hydrochloric Acid → HCID 20135842, 화합물

HRID 580185노트

반응식

HRID 580185 반응식
[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[NH:13][N:12]=2)[CH2:3][CH2:2]1.[ClH:20].C(OCC)C>C(O)C>[ClH:20].[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[NH:13][N:12]=2)[CH2:3][CH2:2]1

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 3065651Indazole, 3-((3-morpholinopropyl)amino)-

생성물 1

HCID 20135842HCID 20135842, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

In 15 ml of absolute ethyl alcohol was dissolved 1.0 g of the 3-(3-morpholinopropylamino)indazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 3-(3-morpholinopropylamino)indazole hydrochloride having the following analytical value.

후처리

  1. temperatureunder cooling with ice
  2. customto separate crystals
  3. customThe crystals were obtained by filtration
  4. customdried

출처 및 근거

ORD 기록
ord-b390ca5c4ea74457b3c9eacb66a1a633
출처 데이터셋
uspto-grants-1988_06
특허 번호
US04751302

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