참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | 4'-Bromoacetanilide | HCID 7683 | — |
| 용매 | Methanesulfonic Acid | HCID 6395 | — |
| 생성물 | N-(4-bromo-2-nitrophenyl)acetamide | HCID 136690 | — |
반응 단계
A solution of 4-bromoacetanilide (20 g, 93.4 mmol) in methanesulfonic acid is cooled to 10° C. Conc. nitric acid (12.6 ml) is added and the mixture is stirred at 40° C. for 2 hours. The mixture is poured into ice-water. The product is filtered off, washed with water and dried. Yield: 23.59 g (97%). Mp 99-100° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05922724 |
|---|
| 출처 데이터셋 | uspto-grants-1999_07 |
|---|
| ORD ID | ord-8d0de64f9359453cae0c0c6038f3b65f |
|---|
| 출처 메모 | uspto-grants-1999_07 |
|---|
