3,3-Diethoxy-1-propanol → 3,3-Diethoxy-1-propanol

HRID 582797노트

반응식

HRID 582797 반응식
[CH2:1]([O:3][CH:4]([O:8][CH2:9][CH3:10])[CH2:5][CH2:6][OH:7])[CH3:2].C1C2C(=CC=CC=2)C=CC=1.[K:21]>O1CCCC1>[K:21].[CH2:1]([O:3][CH:4]([O:8][CH2:9][CH3:10])[CH2:5][CH2:6][OH:7])[CH3:2]

참가 물질

5

반응물 2

HCID 1401353,3-Diethoxy-1-propanolHCID 66602812Naphthalene potassium

생성물 2

HCID 1401353,3-Diethoxy-1-propanolHCID 5462222Potassium

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매2회

실험 절차

THF 20 ml, 3, 3-diethoxypropanol 0.15 g, and a potassium naphthalene 0.5 mol/L-tetrahydrofuran solution 2 ml was added to the reaction container and agitated for 3 minutes in an argon atmosphere; a potassium compound of 3, 3-diethoxypropanol (potassium 3, 3-diethoxypropanoxide) was produced.

출처 및 근거

ORD 기록
ord-be0e5851f18348e5bd356c4e5bd2954b
출처 데이터셋
uspto-grants-1999_07
특허 번호
US05925720

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