Iodoethane → HCID 70053935, 화합물

HRID 583338노트

반응식

HRID 583338 반응식
[CH3:1][O:2][C:3](=[O:24])[C:4]1[CH:9]=[C:8]([CH3:10])[CH:7]=[C:6]([CH3:11])[C:5]=1[NH:12][S:13]([C:16]1[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][CH:17]=1)(=[O:15])=[O:14].[CH2:25](I)[CH3:26]>>[CH3:1][O:2][C:3](=[O:24])[C:4]1[CH:9]=[C:8]([CH3:10])[CH:7]=[C:6]([CH3:11])[C:5]=1[N:12]([CH2:25][CH3:26])[S:13]([C:16]1[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][CH:17]=1)(=[O:15])=[O:14]

참가 물질

3

반응물 2

HCID 6340IodoethaneHCID 53963569HCID 53963569, 화합물

생성물 1

HCID 70053935HCID 70053935, 화합물수율 100%

실험 절차

In the same manner as described in Example 9, 0.30 g (0.860 mmol) of the product of Example 62 was alkylated with ethyl iodide to give 0.324 g (100%) of the desired product as a white solid. Electrospray Mass Spec: 378 (M+H).

출처 및 근거

ORD 기록
ord-ea1e1ab900544e6fba6ac579f2034bde
출처 데이터셋
uspto-grants-1999_07
특허 번호
US05929097

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