Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Formylphenylboronic Acid → HCID 86591268, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Formylphenylboronic Acid | HCID 591073 | — |
| 반응물 | tert-Butyl 3-bromobenzyl(methyl)carbamate | HCID 20738487 | — |
| 생성물 | HCID 86591268 | HCID 86591268 | — |
반응 단계
In a manner similar to that of Example 1(e), by reacting 38 g (127 mmol) of tert-butyl (3-bromo benzyl)-N-methylcarbamate obtained in Example 79(b) with 25.6 g (170 mmol) of 4-formylbenzene boronic acid, and after purification by chromatography on a column of silica eluted with a heptane/ethyl acetate mixture (9/1), 20 g (57%) of the expected product are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06927228B2 |
| 출처 데이터셋 | uspto-grants-2005_08 |
| ORD ID | ord-a89609cff2d8439b9bd4f54bf526b5ef |
| 출처 메모 | uspto-grants-2005_08 |