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[CH:1]1[C:13]2[N:12]([CH:14]3[C:23]4[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=4)[N:17]([C:24](=[O:35])[C:25]4[CH:30]=[CH:29][C:28]([O:31][CH3:32])=[C:27]([O:33][CH3:34])[CH:26]=4)[CH:16]([CH2:36][CH2:37][CH2:38][CH2:39][CH2:40]O)[CH2:15]3)[C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH2:42]([SH:48])[CH2:43][CH2:44][CH2:45][CH2:46][CH3:47]>>[CH3:34][O:33][C:27]1[CH:26]=[C:25]([CH:30]=[CH:29][C:28]=1[O:31][CH3:32])[C:24]([N:17]1[C:18]2[C:23](=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH:14]([N:12]2[C:13]3[CH:1]=[CH:2][CH:3]=[CH:4][C:5]=3[C:6]3[C:11]2=[CH:10][CH:9]=[CH:8][CH:7]=3)[CH2:15][CH:16]1[CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][S:48][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH3:47])=[O:35]참가 물질
3
실험 절차
Starting with 5-[4-(9H-9-carbazolyl)-1-(3,4-dimethoxybenzoyl)-1,2,3,4-tetrahydro-2-quinolinyl]-1-pentanol (0.08 g, 0.15 mmol) prepared in Example 135 and n-hexylmercaptan (0.3 ml), the same procedure as shown in Example 136 was repeated to give the titled compound (0.01 g, yield: 7%) as a white crystal (cis:trans=6:1).
출처 및 근거
- ORD 기록
- ord-22b2ffa25a3a4a679202a7619554e586
- 출처 데이터셋
- uspto-grants-2005_08
- 특허 번호
- US06930104B2
연결된 노트
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