3-Pyridinecarboxaldehyde → HCID 9837985, 화합물

HRID 586569노트

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HRID 586569 반응식
[NH2:1][C:2]1[N:6]=[CH:5][NH:4][N:3]=1.[C:7]([N+:11]#[C-:12])([CH3:10])([CH3:9])[CH3:8].[N:13]1[CH:18]=[CH:17][CH:16]=[C:15]([CH:19]=O)[CH:14]=1>Cl(O)(=O)(=O)=O>[C:7]([NH:11][C:12]1[N:3]2[NH:4][CH:5]=[N:6][C:2]2=[N:1][C:19]=1[C:15]1[CH:14]=[N:13][CH:18]=[CH:17][CH:16]=1)([CH3:10])([CH3:9])[CH3:8]

참가 물질

5

반응물 3

HCID 103713-PyridinecarboxaldehydeHCID 23577Tert-Butyl isocyanideHCID 178418311HCID 178418311, 화합물

생성물 1

HCID 9837985HCID 9837985, 화합물

시약·촉매·용매 1

HCID 24247Perchloric Acid용매

실험 절차

Compound 6 was prepared in accordance with the general synthesis instructions from 1.0 ml (0.1 mmol) 3-amino-1,2,4-triazole solution (0.1 M, MC), 0.575 ml (0.115 mmol) tert-butylisonitrile solution (0.2 M, MC), 0.500 ml (0.15 mmol) 3-pyridinecarbaldehyde solution (0.3 M, MC) and 10 μl perchloric acid (w=20%) in a substance library.

출처 및 근거

ORD 기록
ord-f0095d47fc604f40a01b530808ca5118
출처 데이터셋
uspto-grants-2005_08
특허 번호
US06936631B2

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