Iodoethane → HCID 69737384, 화합물

HRID 586650노트

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HRID 586650 반응식
[CH3:1][O:2][CH2:3][CH:4]1[C@H:6]([CH2:7][OH:8])[C:5]1([CH3:23])[C:9]1[CH:18]=[CH:17][C:16]2[C:15]([CH3:20])([CH3:19])[CH2:14][CH2:13][C:12]([CH3:22])([CH3:21])[C:11]=2[CH:10]=1.[CH2:24](I)C>>[CH2:1]([O:2][CH2:3][CH:4]1[C@H:6]([CH2:7][OH:8])[C:5]1([CH3:23])[C:9]1[CH:18]=[CH:17][C:16]2[C:15]([CH3:20])([CH3:19])[CH2:14][CH2:13][C:12]([CH3:22])([CH3:21])[C:11]=2[CH:10]=1)[CH3:24]

참가 물질

3

반응물 2

HCID 6340IodoethaneHCID 69738373HCID 69738373, 화합물

생성물 1

HCID 69737384HCID 69737384, 화합물수율 78%

실험 절차

Following a procedure similar to that for the preparation of Intermediate 6a using Intermediate 4 as the starting material and ethyl iodide as alkylating reagent yielded the title compound as a colorless oil (69 mg, 78% yield):

출처 및 근거

ORD 기록
ord-195b8beebbae4ac1acdaa614980006b3
출처 데이터셋
uspto-grants-2005_08
특허 번호
US06936636B2

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