Ketene → HCID 131734414, 화합물
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[Cl:1][CH2:2][C:3](=[O:8])[CH2:4][C:5](N)=[O:6].C=C=[O:11]>>[Cl-:1].[Cl:1][CH2:2][C:3](=[O:8])[CH2:4][C:5]([O-:11])=[O:6]참가 물질
3
실험 절차
In a preferred embodiment of the invention, the yield of the 4-chloroacetoaceticacid ester, 4-chloroacetoaceticacid amide or 4-chloroacetoaceticacid imide is at least 90%, based on the total amount of ketene provided in step (a). More preferably, the yield is above 92% or above 95%. Preferably, the yield of 4-chloroacetoacetate chloride obtained in the first reaction step is more than 90%, preferably more than 95% or more than 98%. Preferably, the conversion of chlorine is at least 95%, more preferably at least 98% or at least 99.5%.
출처 및 근거
- ORD 기록
- ord-4e076a0f3c6f4e338eb3d6368cd53185
- 출처 데이터셋
- uspto-grants-2016_01
- 특허 번호
- US09227905B2
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