Ketene → HCID 131734414, 화합물

HRID 587790노트

반응식

HRID 587790 반응식
[Cl:1][CH2:2][C:3](=[O:8])[CH2:4][C:5](N)=[O:6].C=C=[O:11]>>[Cl-:1].[Cl:1][CH2:2][C:3](=[O:8])[CH2:4][C:5]([O-:11])=[O:6]

참가 물질

3

실험 절차

In a preferred embodiment of the invention, the yield of the 4-chloroacetoaceticacid ester, 4-chloroacetoaceticacid amide or 4-chloroacetoaceticacid imide is at least 90%, based on the total amount of ketene provided in step (a). More preferably, the yield is above 92% or above 95%. Preferably, the yield of 4-chloroacetoacetate chloride obtained in the first reaction step is more than 90%, preferably more than 95% or more than 98%. Preferably, the conversion of chlorine is at least 95%, more preferably at least 98% or at least 99.5%.

출처 및 근거

ORD 기록
ord-4e076a0f3c6f4e338eb3d6368cd53185
출처 데이터셋
uspto-grants-2016_01
특허 번호
US09227905B2

반응 노트

불러오는 중…