6-Benzoylbenzoselenazolinone → Bis(2-amino-5-benzoylphenyl) diselenide

HRID 5920노트

반응식

HRID 5920 반응식
[C:1]([C:9]1[CH:18]=[CH:17][C:12]2[N:13]=C[Se:15](=O)[C:11]=2[CH:10]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>[OH-].[Na+]>[NH2:13][C:12]1[CH:17]=[CH:18][C:9]([C:1](=[O:8])[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[CH:10][C:11]=1[Se:15][Se:15][C:11]1[CH:10]=[C:9]([C:1](=[O:8])[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH:18]=[CH:17][C:12]=1[NH2:13]

참가 물질

3

반응물 1

HCID 1317181726-Benzoylbenzoselenazolinone

생성물 1

HCID 10370310Bis(2-amino-5-benzoylphenyl) diselenide

시약·촉매·용매 1

HCID 14798Sodium Hydroxide용매

실험 절차

1.5 g (0.005 mol) of 6-benzoylbenzoselenazolinone are introduced together with 20 cm3 of 10% sodium hydroxide into a ground-necked flask. The mixture is heated to reflux with stirring for two hours. After cooling, the reaction medium is neutralized. The precipitate is drained, washed with water and dried and the product is recrystallized in toluene.

후처리

  1. temperatureThe mixture is heated
  2. temperatureto reflux
  3. temperatureAfter cooling
  4. washwashed with water
  5. customdried
  6. customthe product is recrystallized in toluene

출처 및 근거

ORD 기록
ord-20f53bdf122d4c0eb79fea6119fe9f55
출처 데이터셋
uspto-grants-1993_09
특허 번호
US05246951

반응 노트

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