Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyldithiocarbamic acid, dimethylamine → alpha-(1-Nitroethyl)benzyl dimethyldithiocarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| 반응물 | (2-Nitro-2-propenyl)benzene | HCID 575754 | — |
| 용매 | Carbon Disulfide | HCID 6348 | — |
| 생성물 | alpha-(1-Nitroethyl)benzyl dimethyldithiocarbamate | HCID 21324624 | — |
반응 단계
As in Example 17, reaction of (2-nitro-2-propenyl)benzene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide, gave α-(1-nitroethyl)benzyl dimethyldithiocarbamate melting at 92° C.-94° C. when recrystallized without heating from acetone-ethanol solution.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04011230 |
| 출처 데이터셋 | uspto-grants-1977_03 |
| ORD ID | ord-42b83970ab794375977e587eb15f3827 |
| 출처 메모 | uspto-grants-1977_03 |