Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyldithiocarbamic acid, dimethylamine → 3,4-Dimethoxy-alpha-(nitromethyl)benzyl dimethyldithiocarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| 반응물 | 3,4-Dimethoxy-beta-nitrostyrene | HCID 222093 | — |
| 용매 | Carbon Disulfide | HCID 6348 | — |
| 생성물 | 3,4-Dimethoxy-alpha-(nitromethyl)benzyl dimethyldithiocarbamate | HCID 21324596 | — |
반응 단계
As in Example 17, reaction of 3,4-dimethoxy-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave 3,4-dimethoxy-α-(nitromethyl)-benzyl dimethyldithiocarbamate melting at 108° C.-110° C. after recrystallization without heating from acetone-methanol solution.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04011230 |
| 출처 데이터셋 | uspto-grants-1977_03 |
| ORD ID | ord-3988e83e65054981a44da5047bbc4b0f |
| 출처 메모 | uspto-grants-1977_03 |