Sodium Hydroxide → 1-Amino-2-nitro-4-methoxyethylthiobenzene
반응식
C([NH:4][C:5]1[CH:10]=[CH:9][C:8]([S:11][CH2:12][CH2:13][O:14][CH3:15])=[CH:7][C:6]=1[N+:16]([O-:18])=[O:17])(=O)C.[OH-].[Na+]>CO>[NH2:4][C:5]1[CH:10]=[CH:9][C:8]([S:11][CH2:12][CH2:13][O:14][CH3:15])=[CH:7][C:6]=1[N+:16]([O-:18])=[O:17]참가 물질
4
실험 절차
1.4 G. of 1-acetamido-2-nitro-4-methoxyethylthiobenzene is treated with 3 ml. 5N sodium hydroxide and 6 ml. methanol in the steam bath for about 15 minutes. The mixture is stripped under vacuum and the residue extracted with chloroform. The dried extracts are evaporated giving 1-amino-2-nitro-4-methoxyethylthiobenzene as a red crystalline solid.
후처리
- extractionthe residue extracted with chloroform
- customThe dried extracts are evaporated
출처 및 근거
- ORD 기록
- ord-51ceb430a2114c90a8964a7725cdd469
- 출처 데이터셋
- uspto-grants-1977_03
- 특허 번호
- US04011320
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