Benzylamine → HCID 76073577, 화합물

HRID 59965노트

반응식

HRID 59965 반응식
[CH2:1]([NH2:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.O[C:10]1[C:11]2[CH:19]=[CH:18][CH:17]=[C:16]([C:20]([NH2:22])=[O:21])[C:12]=2[N:13]=[N:14][N:15]=1>>[CH2:1]([NH:8][C:10]1[C:11]2[CH:19]=[CH:18][CH:17]=[C:16]([C:20]([NH2:22])=[O:21])[C:12]=2[N:13]=[N:14][N:15]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 7504BenzylamineHCID 1785136134-oxo-1H-1,2,3-benzotriazine-8-carboxamide

생성물 1

HCID 76073577HCID 76073577, 화합물

실험 절차

Compound 6 was prepared following general synthetic scheme 7 wherein benzylamine was reacted with 4-hydroxybenzo[d][1,2,3]-triazine-8-carboxamide to give the title compound. LC-MS [280 (M+1)], 1H NMR (400 MHz, DMSO-d): δ 9.42 (s, 1H), 9.31 (t, 1H), 8.53 (t, 1H), 8.04 (s, 1H), 7.98 (t, 1H), 7.41 (d, 2H), 7.34 (t, 2H), 7.28-7.24 (m, 1H), 4.92 (d, 2H).

후처리

  1. customCompound 6 was prepared

출처 및 근거

ORD 기록
ord-ca485d4d0227421ebf034cc156c10720
출처 데이터셋
uspto-grants-2016_09
특허 번호
US09440968B2

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