홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Hydrochloric Acid → (1R,2R)-1-Amino-2-phenylcyclopropane-1-carboxylic acid hydrochloride

HRID 600310
노트
인쇄 미리보기

반응식

HRID 600310 반응식
[NH2:1][C@:2]1([C:11]([O:13]C)=[O:12])[CH2:4][C@@H:3]1[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.[ClH:15]>O>[ClH:15].[NH2:1][C@:2]1([C:11]([OH:13])=[O:12])[CH2:4][C@@H:3]1[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 14308470methyl (1R,2R)-1-amino-2-phenylcyclopropane-1-carboxylate

생성물 1

HCID 12336811(1R,2R)-1-Amino-2-phenylcyclopropane-1-carboxylic acid hydrochloride

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A mixture of (1R,2R)-methyl 1-amino-2-phenylcyclopropanecarboxylate (14 mg), water (4 mL) and hydrochloric acid (37% w/v, 6 mL) was heated under reflux for 6 h. The mixture was evaporated to dryness, triturated with diethyl ether and the solid collected and dried to give the subtitle compound (14 mg) as a colourless solid.

후처리

  1. temperaturewas heated
  2. temperatureunder reflux for 6 h
  3. customThe mixture was evaporated to dryness
  4. customtriturated with diethyl ether
  5. customthe solid collected
  6. customdried

출처 및 근거

ORD 기록
ord-2697ca3dc3ed4943a0c8c5e28b7f541c
출처 데이터셋
uspto-grants-2011_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07902181B2

반응 노트

불러오는 중…

이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트