2,6-Dichlorophenol → N-(2',6'-dichlorophenyl)-N-chloroacetyl-4-methylaniline

HRID 603352

반응식

HRID 603352 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1O.[Cl:10][CH2:11][C:12]([NH:14][C:15]1[CH:20]=[CH:19][C:18]([CH3:21])=[CH:17][CH:16]=1)=[O:13]>C1(C)C=CC=CC=1>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[N:14]([C:12](=[O:13])[CH2:11][Cl:10])[C:15]1[CH:16]=[CH:17][C:18]([CH3:21])=[CH:19][CH:20]=1

참가 물질

4

반응물 2

HCID 68992,6-DichlorophenolHCID 279672-Chloro-N-(4-methylphenyl)acetamide

생성물 1

HCID 57952147N-(2',6'-dichlorophenyl)-N-chloroacetyl-4-methylaniline

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Same procedure as example 6a starting from 2,6-dichlorophenol and 2-chloro-N-(4-methylphenyl)acetamide. At the end of the acetylation reaction the mixture was diluted with a small amount of toluene (0.2 part) to prevent solidification.

후처리

  1. customAt the end of the acetylation reaction the mixture

출처 및 근거

ORD 기록
ord-af3bd9ab2c584e5988f942de2ef192e8
출처 데이터셋
uspto-grants-2011_03
특허 번호
US07906677B2

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