Benzylamine → N-benzyl-4-chloro-3-nitrobenzamide

HRID 605085

반응식

[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12].[CH2:14]([NH2:21])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH2:14]([NH:21][C:6](=[O:7])[C:5]1[CH:9]=[CH:10][C:2]([Cl:1])=[C:3]([N+:11]([O-:13])=[O:12])[CH:4]=1)[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

참가 물질

반응물 2

HCID 7504Benzylamine

HCID 1234774-Chloro-3-nitrobenzoyl chloride

생성물 1

HCID 795271N-benzyl-4-chloro-3-nitrobenzamide

실험 절차

A mixture of 4-chloro-3-nitrobenzoyl chloride was reacted with Benzylamine to produce N-Benzyl-4-chloro-3-nitro-benzamide according to the procedure of Example 10A, which was treated sequentially using the procedures from Examples 22A and 22B to provide the title product.

출처 및 근거

ORD 기록: ord-ea526fb59cba499194bfcda3d527093a
출처 데이터셋: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07910595B2

연결된 노트

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