반응식
[ClH:1].[CH3:2][C:3](=[CH:5][CH2:6][CH3:7])[CH3:4].[N:8]([O:10]CCC(C)C)=O>>[Cl:1][C:3]([CH3:4])([CH:5]([N:8]=[O:10])[CH2:6][CH3:7])[CH3:2]참가 물질
4
반응 조건
- 온도
- -20 °C
실험 절차
Dry hydrogen chloride gas was passed into a mixture of 2-methyl-2-pentene (20 g, 237 mmol) and iso-amyl nitrite (55.67 g, 475 mmol) cooled to -20° C. The reaction mixture was left to stir at 0° C. overnight and the precipitated material was then filtered off and washed with cold (-20° C.) ethanol (3×5 ml). The product was dried in a stream of air and was used without further purification, (13 g, 36%).
후처리
- waitThe reaction mixture was left
- filtrationthe precipitated material was then filtered off
- washwashed with cold (-20° C.) ethanol (3×5 ml)
- customThe product was dried in a stream of air
- customwas used without further purification, (13 g, 36%)
출처 및 근거
- ORD 기록
- ord-05e94ea8f0d644f3b3c8be9d4ebb5bb0
- 출처 데이터셋
- uspto-grants-1999_12
- 특허 번호
- US05997843
연결된 노트
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