Hydrochloric Acid → HCID 19600026, 화합물

HRID 611212노트

반응식

HRID 611212 반응식
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([S:14]([CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)(=[O:16])=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:3].[ClH:28]>CO>[ClH:28].[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([S:14]([CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][C:22]3[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=3)(=[O:16])=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:3]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 19599983HCID 19599983, 화합물

생성물 1

HCID 19600026HCID 19600026, 화합물

시약·촉매·용매 1

HCID 887Methanol용매2회

실험 절차

N,N-Dimethyl-[5-(5-phenylpentylsulfonyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.244 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. After this mixture was concentrated, diethyl ether was added; the resulting solid was filtered and washed with diethyl ether to yield the desired product.

후처리

  1. concentrationAfter this mixture was concentrated
  2. additiondiethyl ether was added
  3. filtrationthe resulting solid was filtered
  4. washwashed with diethyl ether

출처 및 근거

ORD 기록
ord-74ff4d90d44447cea414b9d38c3bec47
출처 데이터셋
uspto-grants-1999_12
특허 번호
US05998433

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