Hydrochloric Acid → HCID 19600207, 화합물

HRID 611396노트

반응식

HRID 611396 반응식
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([C:14](=[O:33])[C:15]3[CH:20]=[CH:19][C:18]([C:21]4([C:27]5[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=5)[S:26][CH2:25][CH2:24][CH2:23][S:22]4)=[CH:17][CH:16]=3)[CH2:8][C:7]=2[CH:6]=1)[CH3:3].[ClH:34]>CO.C(OCC)(=O)C>[ClH:34].[CH3:3][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([C:14](=[O:33])[C:15]3[CH:16]=[CH:17][C:18]([C:21]4([C:27]5[CH:28]=[CH:29][CH:30]=[CH:31][CH:32]=5)[S:22][CH2:23][CH2:24][CH2:25][S:26]4)=[CH:19][CH:20]=3)[CH2:8][C:7]=2[CH:6]=1)[CH3:1]

참가 물질

5

반응물 2

HCID 313Hydrochloric AcidHCID 19600032HCID 19600032, 화합물

생성물 1

HCID 19600207HCID 19600207, 화합물

시약·촉매·용매 2

HCID 887Methanol용매HCID 8857Ethyl Acetate용매

실험 절차

N,N-Dimethyl-[5-[4-(2-phenyl-1,3-dithian-2-yl)benzoyl]-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.368 g was dissolved in 2 ml of methanol; hydrogen chloride in ethyl acetate was added in excess, followed by stirring. This mixture was concentrated and washed with diethyl ether to yield the desired product.

후처리

  1. concentrationThis mixture was concentrated
  2. washwashed with diethyl ether

출처 및 근거

ORD 기록
ord-99600573d6154d6d91955846042db291
출처 데이터셋
uspto-grants-1999_12
특허 번호
US05998433

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