Hydrochloric Acid → 2-dimethylaminomethyl-5-(6-phenylhexyl)-6,7-dihydro-5H-furo[3,2-c]pyridin-4-one hydrochloride

HRID 611431노트

반응식

HRID 611431 반응식
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[C:8](=[O:26])[C:7]=2[CH:6]=1)[CH3:3].[ClH:27]>CO>[ClH:27].[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[C:8](=[O:26])[C:7]=2[CH:6]=1)[CH3:3]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 195999812-dimethylaminomethyl-5-(6-phenylhexyl)-6,7-dihydro-5H-furo[3,2-c]pyridin-4-one

생성물 1

HCID 195999802-dimethylaminomethyl-5-(6-phenylhexyl)-6,7-dihydro-5H-furo[3,2-c]pyridin-4-one hydrochloride

시약·촉매·용매 1

HCID 887Methanol용매2회

실험 절차

2-Dimethylaminomethyl-5-(6-phenylhexyl)-6,7-dihydro-5H-furo[3,2-c]pyridin-4-one 0.159 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated; the resulting solid was washed with diethyl ether to yield the desired product.

후처리

  1. concentrationThis mixture was concentrated
  2. washthe resulting solid was washed with diethyl ether

출처 및 근거

ORD 기록
ord-9a234c6418aa446cbd082e10d9c24144
출처 데이터셋
uspto-grants-1999_12
특허 번호
US05998433

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