Potassium Carbonate → HCID 19595683, 화합물

HRID 612583

반응식

HRID 612583 반응식
[OH:1][C:2]1[CH:3]=[C:4]([C:12]([O:14][CH3:15])=[O:13])[C:5](=[CH:10][CH:11]=1)[C:6]([O:8][CH3:9])=[O:7].C(=O)([O-])[O-].[K+].[K+].[CH3:22][O:23][C:24]1[CH:31]=[CH:30][C:27]([CH2:28]Cl)=[CH:26][CH:25]=1>CN(C=O)C>[CH3:22][O:23][C:24]1[CH:31]=[CH:30][C:27]([CH2:28][O:1][C:2]2[CH:3]=[C:4]([C:12]([O:14][CH3:15])=[O:13])[C:5](=[CH:10][CH:11]=2)[C:6]([O:8][CH3:9])=[O:7])=[CH:26][CH:25]=1

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 699934-Methyloxybenzyl chlorideHCID 89726Dimethyl 4-hydroxyphthalate

생성물 1

HCID 19595683HCID 19595683, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

1 eq. of dimethyl 4-hydroxyphthalate, 1.1 eq. of potassium carbonate and 1.1 eq. of 4-methoxybenzyl chloride were stirred in DMF at RT. After 4 days, the mixture was worked up according to a standard procedure. Dimethyl 4-(4-methoxybenzyloxy)phthalate was isolated as a colorless oil. MS: 331 ((M+1)+)

출처 및 근거

ORD 기록
ord-6aa64a686a13461fbdec1ab546ad0f32
출처 데이터셋
uspto-grants-1999_12
특허 번호
US06005010

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