Acrylamide → Prop-2-enamide;styrene
반응식
[Cl-].C[N+](C)(C)CCOC(=O)C=C.[CH2:13]=[CH:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.[C:21]([NH2:25])(=[O:24])[CH:22]=[CH2:23]>C(O)(C)C>[CH2:13]=[CH:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.[C:21]([NH2:25])(=[O:24])[CH:22]=[CH2:23]참가 물질
5
반응 조건
- 온도
- 75 °C
실험 절차
To a 500 mL round-bottom, three-neck flask fitted with a thermocouple, reflux condenser, and septum was added 150 mL of isopropanol followed by 16.13 g of a 50% aqueous solution of 2-trimethylammonioethylacrylate chloride, 8.06 g of styrene, and 8.06 g of acrylamide. The solution was purged with nitrogen for 1 hour and 0.5 g AIBN was added. The mixture was purged for ~ 15 minutes until all of the AIBN dissolved. The solution was heated to 75° C. under nitrogen for 16 hours.
후처리
- customTo a 500 mL round-bottom, three-neck flask fitted with a thermocouple
- temperaturereflux condenser
- customThe solution was purged with nitrogen for 1 hour
- addition0.5 g AIBN was added
- customThe mixture was purged for ~ 15 minutes until all of the AIBN
- dissolutiondissolved
출처 및 근거
- ORD 기록
- ord-0c0d54069c9342cabf35f5871433f414
- 출처 데이터셋
- uspto-grants-1999_12
- 특허 번호
- US06007803
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