N-(2-Chloroethyl)-N-ethylaniline → N,N-dimethyl-N-2-(N'-ethylanilino)ethyl-N-2-hydroxyethylammonium chloride
반응식
[CH3:1][N:2]([CH2:4][CH2:5][OH:6])[CH3:3].[CH2:7]([N:9]([CH2:16][CH2:17][Cl:18])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[CH3:8]>O>[Cl-:18].[CH3:1][N+:2]([CH3:3])([CH2:17][CH2:16][N:9]([CH2:7][CH3:8])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[CH2:4][CH2:5][OH:6]참가 물질
4
실험 절차
A stirred mixture of 35.6 parts of dimethylaminoethanol in 60 parts of water was heated to 90° and 73.6 parts of N-ethyl-N-(2-chloroethyl)aniline was gradually added. The mixture was heated at 90°-95°. After two and one-half hours there are obtained N,N-dimethyl-N-2-(N'-ethylanilino)ethyl-N-2-hydroxyethylammonium chloride in the form of an aqueous solution.
후처리
- temperaturewas heated to 90°
- temperatureThe mixture was heated at 90°-95°
출처 및 근거
- ORD 기록
- ord-d0d7e65d5bac47e785a30cda370c9ef9
- 출처 데이터셋
- uspto-grants-1979_03
- 특허 번호
- US04146558
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