Bis(2-ethylhexyl)amine → 3-bromo-N,N-bis(2-ethylhexyl)propanamide

HRID 61521

반응식

HRID 61521 반응식
[CH3:1][CH2:2][CH2:3][CH2:4][CH:5]([CH2:8][NH:9][CH2:10][CH:11]([CH2:14][CH2:15][CH2:16][CH3:17])[CH2:12][CH3:13])[CH2:6][CH3:7].[Br:18][CH2:19][CH2:20][C:21](Cl)=[O:22]>>[Br:18][CH2:19][CH2:20][C:21]([N:9]([CH2:8][CH:5]([CH2:6][CH3:7])[CH2:4][CH2:3][CH2:2][CH3:1])[CH2:10][CH:11]([CH2:12][CH3:13])[CH2:14][CH2:15][CH2:16][CH3:17])=[O:22]

참가 물질

3

반응물 2

HCID 7791Bis(2-ethylhexyl)amineHCID 84944Propanoyl chloride, 3-bromo-

생성물 1

HCID 1180597233-bromo-N,N-bis(2-ethylhexyl)propanamide수율 97%

실험 절차

Step A is conducted using 2,2′-diethylhexylamine and 3-bromo-propanoyl chloride and leads to 3-bromo-N,N-bis(2-ethylhexyl)propanamide (Yield: 97%) for which the 1H and 13C NMR characterisations are given below:

출처 및 근거

ORD 기록
ord-c74bb6131b8b48b99dac9e901d44e2c4
출처 데이터셋
uspto-grants-2016_09
특허 번호
US09441285B2

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