Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Hydroxy cyclopentyl-acetaldehyde → 3-(2-Hexenyl)-cyclopentanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Hydroxy cyclopentyl-acetaldehyde | HCID 53769794 | — |
| 촉매 | Butyltriphenylphosphonium bromide | HCID 159628 | — |
| 생성물 | 3-(2-Hexenyl)-cyclopentanol | HCID 54157289 | 42.7% |
반응 단계
Using the procedure of Example 3, 5 g of 3-hydroxy cyclopentyl-acetaldehyde and 20 g of triphenyl butyl phosphonium bromide were reacted and the product was chromatographed over silica gel. Elution with a 7-3 cyclohexane-ethyl acetate mixture yielded 1.4 g of 3-(2-hexenyl)-cyclopentanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04501687 |
| 출처 데이터셋 | uspto-grants-1985_02 |
| ORD ID | ord-4cc7bc970b8749cb94668077f684ec93 |
| 출처 메모 | uspto-grants-1985_02 |