反应详情

Using the procedure of Example 3, 5 g of 3-hydroxy cyclopentyl-acetaldehyde and 20 g of triphenyl butyl phosphonium bromide were reacted and the product was chromatographed over silica gel. Elution with a 7-3 cyclohexane-ethyl acetate mixture yielded 1.4 g of 3-(2-hexenyl)-cyclopentanol.

1. customwere reacted
2. customthe product was chromatographed over silica gel
3. washElution with a 7-3 cyclohexane-ethyl acetate mixture