Iodoethane → HCID 20370608, 화합물

반응식

[CH3:1][N:2]([CH3:19])[C:3](=[O:18])[CH:4]([CH3:17])[N:5]1[CH:9]=[C:8](C)[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[N:6]1.[CH2:20](I)C>>[CH3:19][N:2]([CH3:1])[C:3]([C:4]1([N:5]2[CH:9]=[CH:8][C:7]([C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=3)=[N:6]2)[CH2:17][CH2:20]1)=[O:18]

참가 물질

반응물 2

HCID 6340Iodoethane

HCID 20370501N,N-dimethyl-2-(4-methyl-3-phenyl-1H-pyrazol-1-yl)propanamide

생성물 1

HCID 20370608HCID 20370608, 화합물

실험 절차

Following the procedure of Example 95, but substituting α-(2-chloroethyl)-N,N-dimethyl-3-phenylpyrazole-1-acetamide for N,N,α,4-tetramethyl-3-phenylpyrazole-1-acetamide and without addition of ethyl iodide there was obtained N,N-dimethyl-1-(3-phenylpyrazol-1-yl)cyclopropanecarboxamide having a melting point of 96°-99° C.

출처 및 근거

ORD 기록: ord-17f965d9400b433c8f64e65f112a2475
출처 데이터셋: uspto-grants-1978_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04072498

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