Hydrochloric Acid → 4-Phenoxybenzene-1,2-diamine

HRID 616137노트

반응식

HRID 616137 반응식
C([NH:4][C:5]1[CH:10]=[CH:9][C:8]([O:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:7][C:6]=1[NH2:18])(=O)C.Cl>CO>[NH2:4][C:5]1[CH:10]=[CH:9][C:8]([O:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:7][C:6]=1[NH2:18]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 203710941-Acetamido-2-amino-4-phenoxybenzene

생성물 1

HCID 106556434-Phenoxybenzene-1,2-diamine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

1-Acetamido-2-amino-4-phenoxybenzene is treated with hydrochloric acid in aqueous methanol to afford 1,2-diamino-4-phenoxybenzene which, in turn, is reacted with methoxycarbonyl isothiocyanate in accordance with the technique set forth in the third paragraph of Example XIV to afford 1,2-bis(3-methoxycarbonyl-2-thioureido)-4-phenoxybenzene.

출처 및 근거

ORD 기록
ord-bd1c84df3a2d494b9fbf89ce0932367a
출처 데이터셋
uspto-grants-1978_02
특허 번호
US04072696

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