2-Chloroethyldiisopropylammonium chloride → 2-Propanamine, N-(1-methylethyl)-N-(2-(2-(2-methylpropoxy)phenoxy)ethyl)-

HRID 616372노트

반응식

HRID 616372 반응식
[Na].[CH2:2]([O:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[OH:13])[CH:3]([CH3:5])[CH3:4].Cl.[CH:15]([N:18]([CH2:22][CH2:23]Cl)[CH:19]([CH3:21])[CH3:20])([CH3:17])[CH3:16]>C(O)C>[CH2:2]([O:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH2:23][CH2:22][N:18]([CH:19]([CH3:21])[CH3:20])[CH:15]([CH3:17])[CH3:16])[CH:3]([CH3:5])[CH3:4]

참가 물질

5

반응물 3

HCID 779422-Chloroethyldiisopropylammonium chlorideHCID 6911612-IsobutoxyphenolHCID 5360545Sodium

생성물 1

HCID 30426732-Propanamine, N-(1-methylethyl)-N-(2-(2-(2-methylpropoxy)phenoxy)ethyl)-

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The compound was prepared as described in Example 1, using sodium (3.45 g; 150 mmole), o-isobutoxyphenol (12.45 g; 75 mmole) and diisopropylaminoethylchloride hydrochloride (15.0 g; 75 mmole) in 200 ml of ethanol. Yield 11.2 g (51%) of product, boiling at 111°-113° C under a pressure of 0.001 mm.Hg, nD25 : 1.4920.

후처리

  1. customThe compound was prepared

출처 및 근거

ORD 기록
ord-d9826df901224041ac2bf5f085253604
출처 데이터셋
uspto-grants-1978_02
특허 번호
US04073917

반응 노트

불러오는 중…