Methyl iodide → 2,3-Pentanedione, 2-(O-methyloxime)

HRID 617627

반응식

HRID 617627 반응식
CI.[CH3:3][C:4](=[N:9][OH:10])[C:5](=[O:8])[CH2:6][CH3:7].[C:11](=O)([O-])[O-].[K+].[K+]>CC(C)=O>[CH3:11][O:10][N:9]=[C:4]([C:5](=[O:8])[CH2:6][CH3:7])[CH3:3]

참가 물질

5

반응물 3

HCID 6328Methyl iodideHCID 11430Potassium CarbonateHCID 67974532,3-Pentanedione, 2-oxime

생성물 1

HCID 541960112,3-Pentanedione, 2-(O-methyloxime)

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

49.7 g (0.35 mol) of methyl iodide are added dropwise at room temperature to a solution of 40.2 g (0.55 mol) of pentane-2,3-dione 2-oxime and 52.0 g (0.38 mol) of potassium carbonate in 400 ml of acetone, and stirring is continued for 12 hours at this temperature.

출처 및 근거

ORD 기록
ord-56b9c51c8bf34f14bc300d585182814c
출처 데이터셋
uspto-grants-1999_09
특허 번호
US05948932

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