Hydrochloric Acid → Ethyl 3-methylbenzimidate hydrochloride

HRID 617635노트

반응식

HRID 617635 반응식
[C:1]1([CH3:9])[CH:6]=[CH:5][CH:4]=[C:3]([C:7]#[N:8])[CH:2]=1.[ClH:10].[CH2:11]([OH:13])[CH3:12]>>[ClH:10].[CH3:9][C:1]1[CH:2]=[C:3]([CH:4]=[CH:5][CH:6]=1)[C:7](=[NH:8])[O:13][CH2:11][CH3:12]

참가 물질

4

반응물 3

HCID 313Hydrochloric AcidHCID 702EthanolHCID 121043-Tolunitrile

생성물 1

HCID 21938086Ethyl 3-methylbenzimidate hydrochloride

실험 절차

Ethyl 3-methylbenzimidate hydrochloride was synthesized in the same manner as in Reference Example 2. That is, m-tolunitrile (25.2 g, 0.215 mol) was treated with hydrogen chloride in ethanol (250 mL) to give 41.7 g (97%) of the target compound as colorless crystals.

출처 및 근거

ORD 기록
ord-472e9956c224470ca9bd5bd552bcd52d
출처 데이터셋
uspto-grants-1999_09
특허 번호
US05948785

반응 노트

불러오는 중…