Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thioglycerol → 2-(2,3-Dihydroxypropylthio)-3',4',5'-trimethoxyacetophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thioglycerol | HCID 7291 | — |
| 반응물 | 2-Bromo-1-(3,4,5-trimethoxyphenyl)ethanone | HCID 3685732 | — |
| 생성물 | 2-(2,3-Dihydroxypropylthio)-3',4',5'-trimethoxyacetophenone | HCID 21850159 | 94.8% |
반응 단계
Substantially the same procedure as in Reference Example 13 was repeated using 1-mercapto-2,3-propanediol (12.25 g) and 2-bromo-3',4',5'-trimethoxyacetophenone (Compound XIa, 16.39 g) obtained in Reference Example 1 to give 2-(2,3-dihydroxypropylthio)-3',4',5'-trimethoxyacetophenone (Compound IX-13, 17.00 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05952355 |
| 출처 데이터셋 | uspto-grants-1999_09 |
| ORD ID | ord-c4a0210276e6436f93e244fa0651ccb0 |
| 출처 메모 | uspto-grants-1999_09 |