Potassium Carbonate → HCID 19858315, 화합물

HRID 621501노트

반응식

HRID 621501 반응식
[CH3:1][O:2][CH:3]=[CH:4]C.[I:6][CH2:7][CH2:8][OH:9].[C:10](=O)([O-])[O-].[K+].[K+]>P(Cl)(Cl)(Cl)=O>[CH3:1][O:2][C:3]([O:9][CH2:8][CH2:7][I:6])([CH3:4])[CH3:10]

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 12225IodoethanolHCID 1112901-Propene, 1-methoxy-

생성물 1

HCID 19858315HCID 19858315, 화합물

시약·촉매·용매 1

HCID 24813Phosphorus oxychloride촉매

실험 절차

To 6 mls of cold (0° C.) methoxypropene was added 3 mls of 2-iodoethanol and 1 drop of phosphorous oxychloride (POCl3). The reaction was stirred for 1 hour and then solid potassium carbonate was added. After 10 minutes the liquid was decanted and concentrated to give the product as an oil.

후처리

  1. customAfter 10 minutes the liquid was decanted
  2. concentrationconcentrated

출처 및 근거

ORD 기록
ord-96a9a1d08ed443f8b99ee43952048400
출처 데이터셋
uspto-grants-1989_04
특허 번호
US04824849

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