반응식
[CH3:1][NH:2][S:3]([CH3:6])(=[O:5])=[O:4].C([Li])CCC.[F:12][C:13]1[CH:22]=[CH:21][C:16]([C:17](OC)=[O:18])=[C:15]([NH:23][CH3:24])[CH:14]=1>>[F:12][C:13]1[CH:22]=[CH:21][C:16]([C:17](=[O:18])[CH2:6][S:3](=[O:5])(=[O:4])[NH:2][CH3:1])=[C:15]([NH:23][CH3:24])[CH:14]=1참가 물질
4
실험 절차
In a similar manner to that described in Example 12(a), N-methylmethanesulphonamide was reacted with n-butyl lithium and the product reacted with methyl 4-fluoro-2-methylaminobenzoate to give the novel compound 1-(4-fluoro-2-methylaminophenyl)-2-(N-methylsulphamoyl)ethanone, m.p. 140°-142°.
출처 및 근거
- ORD 기록
- ord-63e621efc46e492b838d0e66c85af94a
- 출처 데이터셋
- uspto-grants-1988_09
- 특허 번호
- US04772614
연결된 노트
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